HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Toluenesulfonyl chloride → HCID 86621618, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Reactant | HCID 68442963 | HCID 68442963 | — |
| Solvent | Ethylacetate heptane | HCID 21899848 | — |
| Product | HCID 86621618 | HCID 86621618 | — |
Reaction Steps
Similar to example 24c, 9.43 g of (2S)-4,6-dioxo-piperidine-1,2-dicarboxylic acid 2-benzyl ester 1-tert-butyl ester [176436-10-5] are reacted with p-toluene sulfonyl chloride to afford the title compound as a yellow oil Rf=0.64 (EtOAc-heptane 1:1); Rt=5.20.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07687495B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-a5701c1790254c3fa8f9faa19f472ccb |
| Source note | uspto-grants-2010_03 |