2-Morpholinoethylamine → HCID 10207250, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of N-(3,4-dichlorophenyl){6-chloro-2-[(4-pyridylmethyl)amino](3-pyridyl)}carboxamide (18 mg, 0.044 mmol, made from 2,6-dichloronicotinic acid) and 2-morpholin-4-ylethylamine (300 μL) was stirred at 80° C. for 20 h. The reaction mixture was purified on silica gel chromatography to yield N-(3,4-dichlorophenyl){6-[(2-morpholin-4-ylethyl)amino]-2-[(4-pyridylmethyl)-amino](3-pyridyl)}carboxamide. MS (ES+):501 (M+H)+; (ES−):499 (M−H)−. Calc'd for C24H26Cl2N6O2—500.15.

Provenance & Evidence