Ethanol → HCID 59218899, compound

Participants

Reaction Steps

379mg of 3-(2-cyano-4-pyridyl)benzoate, 350 mg of t-butyl dicarbonate and 300 mg of 10% palladium-carbon were added to and dissolved in 16 ml of ethanol and 2 ml of ethyl acetate, and the mixture was stirred at room temperature for 3 hours in a hydrogen atmosphere. The reaction mixture was filtered, and the filtrate was evaporated. The residue was purified by silica gel column, to give 243 mg of the title compound in the 1:1 hexane-ethyl acetate fraction.

Provenance & Evidence