Iodoethane → HCID 59218994, compound

Participants

Reaction Conditions

Reaction Steps

170 mg of Methyl 3-(3-{[(t-butoxycarbonyl)amino]-methyl}-4-hydroxyphenyl)-6-methylbenzoate was dissolved in 5 ml of acetonitrile, 0.5 ml of iodoethane and 500 mg of cesium carbonate were added successively thereto and the mixture was stirred overnight at 50° C. The reaction mixture was diluted with ethyl acetate and successively washed with water and brine, dried over magnesium sulfate, filtered, and the solvent was concentrated, to give 185 mg of the title compound.

Provenance & Evidence