HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 54074111, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 12720680 | HCID 12720680 | — |
| Product | HCID 54074111 | HCID 54074111 | 90.3% |
Reaction Steps
152 g of the 4,4-dichlorobut-3-ene-1-carboxylic acid is stirred with 140 g of thionyl chloride for 2 hours. The subsequent distillation yields 152.3 g of 4,4-dichlorobut-3-ene-1-carboxylic acid chloride; b.p. 62° C./15 Torr [b.p. 64°-65° C./11 Torr according to J. Ray and R. Vessiere, Bull. Soc. Chim. France, 269 (1967)].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04234517 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-779b14e708a342859a50fe4336eef693 |
| Source note | uspto-grants-1980_11 |