HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 14723166, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 14723163 | HCID 14723163 | — |
| Product | HCID 14723166 | HCID 14723166 | — |
Reaction Steps
In the reduction with sodium borohydride a mixture of the desired compound and 1,1-diethyl-3-(2-isopropenyl- 6-n-propyl-8α-ergolinyl)-urea) was produced. Therefore the raw mixture was further reduced with Na/NH3 (see example 12). Yield after crystallization (ethyl acetate): 28%, [α]D +17.6° (c=0.5 in chloroform).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05037832 |
| Source dataset | uspto-grants-1991_08 |
| ORD ID | ord-3a5e9c75643748cb865975096fbe12cd |
| Source note | uspto-grants-1991_08 |