Methyl iodide → HCID 178504016, compound
Reaction equation
[CH3:1][N:2]1[C:6]([NH:7][C:8]([NH2:10])=[S:9])=[CH:5][C:4]([CH3:11])=[N:3]1.[CH3:12][I:13]>>[IH:13].[CH3:1][N:2]1[C:6]([NH:7][C:8](=[NH:10])[S:9][CH3:12])=[CH:5][C:4]([CH3:11])=[N:3]1Participants
3
Procedure
(1,3-Dimethyl-5-pyrazolyl) thiourea (17.0 g) and 14.2 g methyl iodide were reacted as described in Example V to give 18.0 g. of the product, mp 158°-161° C.
Workup
- customto give 18.0 g
Sources & evidence
- ORD record
- ord-73de767ba54b4bcda95994f452708989
- Source dataset
- uspto-grants-1980_11
- Patent number
- US04234594
Reaction notes
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