Ethyl isocyanate → HCID 14552618, compound

HRID 2248170Notes

Reaction equation

[CH3:1][CH:2]([S:5][C:6]1[CH:15]=[CH:14][C:9]([O:10][CH2:11][CH2:12][OH:13])=[CH:8][CH:7]=1)[CH2:3][CH3:4].[CH2:16]([N:18]=[C:19]=[O:20])[CH3:17]>>[CH2:16]([NH:18][C:19](=[O:20])[O:13][CH2:12][CH2:11][O:10][C:9]1[CH:14]=[CH:15][C:6]([S:5][CH:2]([CH3:1])[CH2:3][CH3:4])=[CH:7][CH:8]=1)[CH3:17]

Participants

Reactant 2

HCID 8022Ethyl isocyanate

HCID 14852817HCID 14852817, compound

Product 1

HCID 14552618HCID 14552618, compound

Procedure

Following the above procedure, 2-[4-(1-methylpropylthio)phenoxy]ethanol (2.16 g, 10.0 mmol) is reacted with ethyl isocyanate (1.5 ml, 18.0 mmol) to give O-2-[4-(1-methylpropylthio)phenoxy]ethyl N-ethylcarbamate (compound 39, Table A).

Sources & evidence

ORD record: ord-f1528ab64da64d8e9308544298dba7ae
Source dataset: uspto-grants-1991_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05037991

Reaction notes

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