Ethyl chloroformate → HCID 14552621, compound

HRID 2248174Notes

Reaction equation

HRID 2248174 reaction equation
[CH3:1][C:2]([CH3:16])=[CH:3][CH2:4][S:5][C:6]1[CH:15]=[CH:14][C:9]([O:10][CH2:11][CH2:12][NH2:13])=[CH:8][CH:7]=1.Cl[C:18]([O:20][CH2:21][CH3:22])=[O:19]>>[CH3:1][C:2]([CH3:16])=[CH:3][CH2:4][S:5][C:6]1[CH:15]=[CH:14][C:9]([O:10][CH2:11][CH2:12][NH:13][C:18](=[O:19])[O:20][CH2:21][CH3:22])=[CH:8][CH:7]=1

Participants

3

Reactant 2

HCID 10928Ethyl chloroformateHCID 15662553HCID 15662553, compound

Product 1

HCID 14552621HCID 14552621, compound

Procedure

Following the procedure of Example 13, 2-[4-(3-methyl-2-butenylthio)phenoxy]ethylamine is prepared and is reacted with ethyl chloroformate to give ethyl N-{2-[4-(3-methyl-2-butenylthio)phenoxy]ethyl}carbamate (compound 43, Table A).

Workup

  1. customis prepared

Sources & evidence

ORD record
ord-e4b6b03649e649deb48e06f8a9718d55
Source dataset
uspto-grants-1991_08
Patent number
US05037991

Reaction notes

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