Chlorine → HCID 70591660, compound

HRID 224819Notes

Reaction equation

HRID 224819 reaction equation
[CH3:1][N:2]1[C:6]([NH:7][C:8]2[NH:9][CH2:10][CH2:11][N:12]=2)=[CH:5][CH:4]=[N:3]1.[Cl:13]Cl>C(O)(=O)C>[ClH:13].[Cl:13][C:5]1[CH:4]=[N:3][N:2]([CH3:1])[C:6]=1[NH:7][C:8]1[NH:9][CH2:10][CH2:11][N:12]=1

Participants

4

Reactant 2

HCID 24526ChlorineHCID 12763813HCID 12763813, compound

Product 1

HCID 70591660HCID 70591660, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

2(1-Methyl-5-pyrazolyl) amino-2-imidazoline (15.74 g.) was treated with 2.60 g. chlorine gas in 30 ml. acetic acid, while cooling in ice, by the method of Example VII to give 6.34 g. mp 254°-257°.

Workup

  1. customto give 6.34 g

Sources & evidence

ORD record
ord-48714199de10497d9cd2947297b60134
Source dataset
uspto-grants-1980_11
Patent number
US04234594

Reaction notes

Loading…