HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2[1-(2-Chlorophenyl)-5-pyrazolyl] amino-2-imidazoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1-Acetyl-2[1-(2-chlorophenyl)-5-pyrazolyl] amino-2-imidazoline | HCID 12763793 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2[1-(2-Chlorophenyl)-5-pyrazolyl] amino-2-imidazoline | HCID 12763814 | — |
Reaction Steps
1-Acetyl-2[1-(2-chlorophenyl)-5-pyrazolyl] amino-2-imidazoline (14.0 g.) was treated with HCl in methanol as described in Example II to give 11.10 g. product mp 185°-188° (crystallized from CH3CN)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04234594 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-40fae2e2a6b94d6abf60d423d3c674cc |
| Source note | uspto-grants-1980_11 |