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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2248256Generated: October 30, 2026

Dichloromethane → HCID 86744981, compound

https://huagongshe.com/reaction/2248256

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDichloromethaneHCID 6344—
Reactant3,4-dihydro-2H-pyranHCID 8080—
ReactantHCID 14624888HCID 14624888—
ProductHCID 86744981HCID 86744981—

Reaction Steps

2.00 g of 4-chloro-2-fluoro-5-mercaptophenylisothiocyanate was dissolved in 20 ml of dichloromethane, and 0.77 g of dihydropyran was added thereto. Two hours later dichloromethane was distilled off to obtain 2.77 g of the above-identified compound as yellow oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05039331
Source datasetuspto-grants-1991_08
ORD IDord-c93d03a34d724a10ab3784811296749a
Source noteuspto-grants-1991_08