HCID 15591815, compound → HCID 12763795, compound

HRID 224826Notes

Reaction equation

HRID 224826 reaction equation
Cl.[NH2:2][C:3]1[N:7]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[N:6]=[C:5]([CH3:14])[CH:4]=1.[C:15]([N:18]1[CH2:22][CH2:21][N:20]=[CH:19]1)(=[O:17])[CH3:16]>>[C:15]([N:18]1[CH2:22][CH2:21][N:20]=[C:19]1[NH:2][C:3]1[N:7]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[N:6]=[C:5]([CH3:14])[CH:4]=1)(=[O:17])[CH3:16]

Participants

3

Reactant 2

HCID 15591815HCID 15591815, compoundHCID 2029777578119-06-9

Product 1

HCID 12763795HCID 12763795, compound

Procedure

5-Amino-3-methyl-1-phenyl pyrazole hydrochloride (37.8 g.) and -1-acetyl-2-imidazoline (27.4 g.) were reacted as described in Example I to give 35.4 g. product. mp 153°-162° (crystallized from CH3CN)

Workup

  1. customto give 35.4 g
  2. custommp 153°-162° (crystallized from CH3CN)

Sources & evidence

ORD record
ord-b5a9b93bdfce451e9cf43afe91fcc5f7
Source dataset
uspto-grants-1980_11
Patent number
US04234594

Reaction notes

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