HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl chloroformate → HCID 14232111, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 10797035 | HCID 10797035 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 14232111 | HCID 14232111 | — |
Reaction Steps
To a solution containing 9 g of N-(1H-pyrrol-1-yl)-4-pyridinamine and 15 g of sodium bicarbonate in 350 ml of dichloromethane was added a solution containing 6.7 g of ethyl chloroformate in 50 ml of dichloromethane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05039687 |
| Source dataset | uspto-grants-1991_08 |
| ORD ID | ord-491509a750714228b4fca93e2390ab3d |
| Source note | uspto-grants-1991_08 |