HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 5-bromofuran-2-carboxylate → HCID 19996108, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 5-bromofuran-2-carboxylate | HCID 599633 | — |
| Reactant | HCID 19996123 | HCID 19996123 | — |
| Product | HCID 19996108 | HCID 19996108 | 40.6% |
Reaction Steps
Methyl 5-bromo-2-furancarboxylate (1.49 g) was treated with 3-[(5-bromopentyl)oxy]-1-propyne (1.49 g) according to the method of Intermediate 9 to give the title compound as a yellow oil (0.97 g), t.l.c. (cyclohexane-diethyl ether 10:1) Rf 0.18.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05039697 |
| Source dataset | uspto-grants-1991_08 |
| ORD ID | ord-ef13eaf0e8b445c6b27da093367c7c26 |
| Source note | uspto-grants-1991_08 |