HCID 54135160, compound → HCID 53699739, compound

HRID 2248396Notes

Reaction equation

HRID 2248396 reaction equation
[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH:6]=[CH:7][CH2:8][CH2:9][CH2:10][C:11](O)=[O:12]>CCOCC>[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH:6]=[CH:7][CH2:8][CH2:9][CH2:10][CH2:11][OH:12]

Participants

3

Reactant 1

HCID 54135160HCID 54135160, compound

Product 1

HCID 53699739HCID 53699739, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

6-(2-Furyl)-5-hexenoic acid (3.6 g) in ether (25 ml) was reduced according to the method of Intermediate 15, except that the reaction time was 1.5 h, and there was no purification by FCC. The title compound was obtained as a pale yellow oil (2.89 g), t.l.c. (hexane-ether 1:1) Rf 0.17.

Workup

  1. customno purification by FCC

Sources & evidence

ORD record
ord-c389744d9fe741e2a76e7aa66bc4626d
Source dataset
uspto-grants-1991_08
Patent number
US05039697

Reaction notes

Loading…