1-Aminoindole → HCID 14988267, compound

HRID 2248476Notes

Reaction equation

HRID 2248476 reaction equation
[N:1]1([NH2:10])[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[CH:3]=[CH:2]1.Cl[C:12]1[CH:17]=[CH:16][N:15]=[CH:14][C:13]=1[N+:18]([O-:20])=[O:19]>C(O)C>[N+:18]([C:13]1[CH:14]=[N:15][CH:16]=[CH:17][C:12]=1[NH:10][N:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[CH:3]=[CH:2]1)([O-:20])=[O:19]

Participants

4

Reactant 2

HCID 6432211-AminoindoleHCID 27357814-Chloro-3-nitropyridine

Product 1

HCID 14988267HCID 14988267, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The title compound was prepared from 1H-indol-1-amine and 4-chloro-3-nitropyridine in ethanol at 70° C. for 3 hours in substantially the same manner as in Example 1. Recrystallized from ethanol, m.p. 170°-172° C.

Workup

  1. customRecrystallized from ethanol, m.p. 170°-172° C.

Sources & evidence

ORD record
ord-2366a88b9fe543249d9bda116a65dddc
Source dataset
uspto-grants-1991_08
Patent number
US05039811

Reaction notes

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