HCID 19996313, compound → HCID 19996390, compound

Participants

Reaction Steps

1.43 g of N-[m-[7-(1-t-butoxyformamido)heptanamido]benzoyl]-β-alanine benzyl ester and 476 mg of Pd/C are stirred in 28 ml of formic acid for 5 hours under hydrogen. The reaction mixture is filtered and the filtrate is evaporated in a vacuum. The residue is taken up in water and evaporated. 464 mg of N-[m-(7-aminoheptanamido)benzoyl]-β-alanine, m.p. 236° C., are obtained from methanol.

Provenance & Evidence