HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → N,N'-Bis(2-hydroxyethyl)-2-nitro-p-phenylenediamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 178516900 | HCID 178516900 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N,N'-Bis(2-hydroxyethyl)-2-nitro-p-phenylenediamine | HCID 5488740 | 90% |
Reaction Steps
0.2 mole (53.4 g) of N-[4-(β-hydroxyethyl)amino-3-nitrophenyl]oxazolidone, prepared according to Example 5, is treated with 135 ml of 3N sodium hydroxide to which 55 ml of 96° strength ethanol has been added. 0.18 mole (44.2 g) of the expected product is obtained. It melts at 107° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05041143 |
| Source dataset | uspto-grants-1991_08 |
| ORD ID | ord-295ed4f18b174965a363878bb5981636 |
| Source note | uspto-grants-1991_08 |