Methyl iodide → 131988-14-2

HRID 2248646Notes

Reaction equation

HRID 2248646 reaction equation
[CH3:1][I:2].[CH2:3]([O:7][C:8]1[C:9]([C:13]2[CH:14]=[N:15][CH:16]=[CH:17][CH:18]=2)=[N:10][S:11][N:12]=1)[CH2:4][CH2:5][CH3:6]>CC(C)=O>[I-:2].[CH2:3]([O:7][C:8]1[C:9]([C:13]2[CH:14]=[N+:15]([CH3:1])[CH:16]=[CH:17][CH:18]=2)=[N:10][S:11][N:12]=1)[CH2:4][CH2:5][CH3:6]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 15180133HCID 15180133, compound

Product 1

HCID 19075249131988-14-2

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.3 ml, 5 mmol) and 3-(4-butoxy-1,2,5-thiadiazol-3-yl)pyridine (580 mg, 2.5 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.60 g (64%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 0.60 g (64%)

Sources & evidence

ORD record
ord-52310749dd024921a71a1046d2834129
Source dataset
uspto-grants-1991_08
Patent number
US05041455

Reaction notes

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