Methyl iodide → HCID 70144872, compound

HRID 2248691Notes

Reaction equation

HRID 2248691 reaction equation
[CH3:1][I:2].[CH2:3]([O:9][C:10]1[C:11]([C:15]2[CH:16]=[N:17][CH:18]=[CH:19][CH:20]=2)=[N:12][S:13][N:14]=1)/[CH:4]=[CH:5]\[CH2:6][CH2:7][CH3:8]>CC(C)=O>[I-:2].[CH2:3]([O:9][C:10]1[C:11]([C:15]2[CH:16]=[N+:17]([CH3:1])[CH:18]=[CH:19][CH:20]=2)=[N:12][S:13][N:14]=1)/[CH:4]=[CH:5]\[CH2:6][CH2:7][CH3:8]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 70144708HCID 70144708, compound

Product 1

HCID 70144872HCID 70144872, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.5 ml, 7.5 mmol) and cis-3-(4-(2-hexenyloxy)-1,2,5-thiadiazol-3-yl)pyridine (3 mmol) in acetone (4 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration.

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration

Sources & evidence

ORD record
ord-6cd2cb294f0447ddb4fa7248d88b6f4d
Source dataset
uspto-grants-1991_08
Patent number
US05041455

Reaction notes

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