HuagongsheHuagongshe Chemistry Print Report · For research reference only
ethyl (2Z)-3-(pyridin-3-yl)but-2-enoate → HCID 12727116, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | ethyl (2Z)-3-(pyridin-3-yl)but-2-enoate | HCID 67402107 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12727116 | HCID 12727116 | 95.5% |
Reaction Steps
Ethyl 3-(3-pyridyl)crotonate (13.2 g) was hydrogenated in ethanol (130 ml) at 270 kPa with 10% palladium on charcoal catalyst for 3 hours at room temperature to give ethyl 3-(3-pyridyl)butyrate (12.74 g), b.p. 74°-80°/0.15 mmHg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04234588 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-7fd8f1cbaf3045d08c7dc0e28e79b68d |
| Source note | uspto-grants-1980_11 |