Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl 3-(6-methoxy-3-pyridyl)acrylate → Ethyl 3-(6-methoxy-3-pyridyl)propionate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl 3-(6-methoxy-3-pyridyl)acrylate | HCID 53930754 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Ethyl 3-(6-methoxy-3-pyridyl)propionate | HCID 12799555 | 100.2% |
반응 단계
Ethyl 3-(6-methoxy-3-pyridyl)acrylate (32.33 g) in ethanol (160 ml) was hydrogenated at 344 kPa at 40°. using palladium-on-charcoal catalyst (5%, 0.2 g). The mixture was filtered and the filtrate was evaporated to give ethyl 3-(6-methoxy-3-pyridyl)propionate (32.7 g) as an oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04234588 |
| 출처 데이터셋 | uspto-grants-1980_11 |
| ORD ID | ord-0ef96d1c32504857814c701b6f0cd892 |
| 출처 메모 | uspto-grants-1980_11 |