HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 19994772, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-[(Quinolin-2-yl)methoxy]phenol | HCID 10988737 | — |
| Reactant | HCID 19994725 | HCID 19994725 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 19994772 | HCID 19994772 | — |
Reaction Steps
1.0 g of 4-(2-quinolinylmethyloxy)phenol, .9 g of 7-bromomethyl-2-cyanobenzoxazole and 0.5 g of potassium carbonate are stirred at room temperature in 5 ml of dimethylformamide for 2 days. The reaction mixture is diluted with ethylacetate, filtered and concentrated. The residue is chromatographed on silica gel to give 2-cyano-7-(4-(quinolin-2-ylmethyloxy)phenoxymethyl)benzoxazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05041453 |
| Source dataset | uspto-grants-1991_08 |
| ORD ID | ord-c801153355da49e18a3c8f676cc425ba |
| Source note | uspto-grants-1991_08 |