2-Nitropropane → 5-methoxy-3-(2,2-dimethyl-2-nitroethyl)-1H-indole

Beteiligte Stoffe

Reaktionsschritte

This material was prepared by the reaction of 5-methoxygramine (Procedure 69B) and 2-nitropropane substantially as described in Procedure 67C. The product was initially recovered as a dark oil which crystallized from i-Pr2O solution after treatment thereof with activated carbon, yield 31.3 g. (from 33 g. of 5-methoxygramine), m.p. 83°-85°. The identity of the product was confirmed by inspection of its NMR spectrum.

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