HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(5-Phenoxypent-1-ynyl)benzyl alcohol → 4-(5-Phenoxypentyl)benzyl alcohol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(5-Phenoxypent-1-ynyl)benzyl alcohol | HCID 14576781 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-(5-Phenoxypentyl)benzyl alcohol | HCID 14576782 | 98% |
Reaction Steps
A solution of 0.54 g of 4-(5-phenoxy-1-pentyn-1-yl)benzyl alcohol in 100 ml methanol was treated with 230 mg of 5% palladium on charcoal and 58 PSI hydrogen for 3.5 hours. The product mixture was filtered using celite and the filtrate was evaporated in vacuo to yield 0.53 g of the compound in the heading in the form of a light tan solid which was used without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05041638 |
| Source dataset | uspto-grants-1991_08 |
| ORD ID | ord-f12228a9c67543c78302e7c694658f55 |
| Source note | uspto-grants-1991_08 |