Methyl iodide → HCID 19075349, compound

HRID 2249184Notes

Reaction equation

HRID 2249184 reaction equation
[CH3:1][I:2].[CH2:3]([O:7][C:8]1[C:9]([C:13]2[CH:14]=[N:15][CH:16]=[CH:17][CH:18]=2)=[N:10][S:11][N:12]=1)[CH2:4][CH:5]=[CH2:6]>CC(C)=O>[I-:2].[CH2:3]([O:7][C:8]1[C:9]([C:13]2[CH:14]=[N+:15]([CH3:1])[CH:16]=[CH:17][CH:18]=2)=[N:10][S:11][N:12]=1)[CH2:4][CH:5]=[CH2:6]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 19075515HCID 19075515, compound

Product 1

HCID 19075349HCID 19075349, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.5 ml, 7.5 mmol) and 3-(4-(3-butenyloxy)-1,2,5-thiadiazol-3-yl)pyridine (583 mg, 2.5 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 890 g (96%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 890 g (96%)

Sources & evidence

ORD record
ord-6aa10ffe14784ea8b5c7286eee9413f9
Source dataset
uspto-grants-1991_08
Patent number
US05043345

Reaction notes

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