HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dibenzylamine → 1,1-dibenzylurea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dibenzylamine | HCID 7656 | — |
| Reactant | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | 1,1-dibenzylurea | HCID 236154 | 62% |
Reaction Steps
As described in Example 6, but using a 20strength solution of dibenzylamine in N-methylpyrrolidone instead of dodecylamine at a temperature of 70 C, N,N dibenzylurea was obtained in a yield of 62% of theory after recrystallizing from water/acetone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05043444 |
| Source dataset | uspto-grants-1991_08 |
| ORD ID | ord-d78ea9247eb14b9eae2d7945f9aa3ad5 |
| Source note | uspto-grants-1991_08 |