HCID 23094122, compound → HCID 23094142, compound

HRID 2249433Notes

Reaction equation

HRID 2249433 reaction equation
ClC1C=CC(CCCN2C(=O)C(CN3CCN(C)CC3)=CC(C3C=CC4OCCC=4C=3)=N2)=CC=1.[C:35]([C:38]1[C:39](=[O:61])[N:40]([CH2:53][C:54]2[CH:59]=[CH:58][CH:57]=[CH:56][C:55]=2[Cl:60])[N:41]=[C:42]([C:44]2[CH:45]=[CH:46][C:47]3[O:51][CH2:50][CH2:49][C:48]=3[CH:52]=2)[CH:43]=1)(O)=[O:36]>>[Cl:60][C:55]1[CH:56]=[CH:57][CH:58]=[CH:59][C:54]=1[CH2:53][N:40]1[C:39](=[O:61])[C:38]([CH2:35][OH:36])=[CH:43][C:42]([C:44]2[CH:45]=[CH:46][C:47]3[O:51][CH2:50][CH2:49][C:48]=3[CH:52]=2)=[N:41]1

Participants

3

Reactant 2

HCID 23094122HCID 23094122, compoundHCID 23094133HCID 23094133, compound

Product 1

HCID 23094142HCID 23094142, compound

Procedure

The general procedure of Example 1 (4) was repeated by use of 4-carboxy-2-(2-chlorobenzyl)-6-(2,3-dihydro-1-benzofuran-5-yl)-2H-pyridazin-3-one, to thereby yield the title compound as pale yellow needle-like crystal (yield: 42.8%).

Sources & evidence

ORD record
ord-f8da11c324aa4a7b9ad59040e8d5cfe8
Source dataset
uspto-grants-2008_01
Patent number
US07314877B2

Reaction notes

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