HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosulfonic acid → HCID 135856749, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosulfonic acid | HCID 24638 | — |
| Reactant | 2-(2-Ethoxyphenyl)-5-ethyl-7-propylimidazo[5,1-f][1,2,4]triazin-4(1H)-one | HCID 135856757 | — |
| Product | HCID 135856749 | HCID 135856749 | — |
Reaction Steps
At 0° C., 1.70 g (5.21 mmol) of 2-(2-ethoxy-phenyl)-5-ethyl-7-propyl-3H-imidazo[5,1-f][1,2,4]triazin-4-one are added slowly to 3.12 ml of chlorosulphonic acid. The reaction mixture is stirred at room temperature overnight and then poured into ice-water and extracted with dichloromethane. This gives 2.10 g (94%) of a colourless foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07314871B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-5093aa35f33a4ee89e18a0a6dbf315ba |
| Source note | uspto-grants-2008_01 |