HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 178485044, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 178503914 | HCID 178503914 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178485044 | HCID 178485044 | — |
Reaction Steps
To a solution of 2-guanidino-4-[5-(3-cyano-2-methylisothioureido)pentyl]thiazole in ethanol was added ethanolic methylamine (33% w/v, 15 ml.). The mixture was allowed to stand overnight and then evaporated to dryness. The residue was crystallized from acetonitrile to give 2-guanidino-4-[5-(2-cyano-3-methylguanidino)pentyl]thiazole, m.p. 109°-113° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04234735 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-1ad39bef956b4808a7dae585d71e453d |
| Source note | uspto-grants-1980_11 |