HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyldichlorosilane → HCID 123155376, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyldichlorosilane | HCID 6376 | — |
| Reactant | Dicyclopentadiene | HCID 6492 | — |
| Reactant | Hexadecane | HCID 11006 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 123155376 | HCID 123155376 | 781.2% |
Reaction Steps
As described in Example 2, 1.49 g (0.0113 mol) of dicyclopentadiene, 10.79 g (0.0902 mol) of methyldichlorosilane, 5 mL of toluene and 2 mL of hexadecane were placed in a reactor. The reactor was sealed and the reaction was performed at 250° C. for 1 hour. Products were subject to simple vacuum distillation, thereby providing a mixture (15.99 g) of (2-cyclopentenyl)methyldichlorosilane (1.2 g, 29%), unreacted methyldichlorosilane, toluene and hexadecane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07314946B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-7bd6858485af426a87d275d9711c7875 |
| Source note | uspto-grants-2008_01 |