Methyldichlorosilane → HCID 123155376, compound

Participants

Reaction Steps

As described in Example 2, 2.87 g (0.0217 mol) of dicyclopentadiene, 3.74 g (0.0326 mol) of methyldichlorosilane, 0.036 g (0.000203 mol) of palladium dichloride, 100 μL (0.000406 mol) of tributylphosphine, 4 mL of toluene and 2 mL of hexadecane were placed in a reactor. The reactor was sealed and the reaction was performed at 180° C. for 1 hour. Products were subject to simple vacuum distillation, thereby providing a mixture (11.4 g) of (2-cyclopentenyl)methyldichlorosilane (4.3 g, 72%), other unreacted reactants, toluene, hexadecane, and unidentified compounds.

Provenance & Evidence