Methyldichlorosilane → HCID 123155376, compound

Participants

Reaction Steps

As described in Example 2, 3.01 g (0.0228 mol) of dicyclopentadiene, 5.19 g (0.0451 mol) of methyldichlorosilane, 0.032 g (0.000247 mol) of nickel dichloride, 57 μL (0.000230 mol) of tributylphosphine and 4 mL of toluene and 2 mL of hexadecane were placed in a reactor. The reactor was sealed and the reaction was performed at 180° C. for 1 hour. Products were subject to simple vacuum distillation, thereby providing a mixture (11.8 g) of (2-cyclopentenyl)methyldichlorosilane (3.1 g, 38%), other unreacted reactants, toluene, hexadecane, and unidentified compounds.

Provenance & Evidence