HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 4-methylidenecyclohexane-1-carboxylate → 4-Methylenecyclohexylmethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 4-methylidenecyclohexane-1-carboxylate | HCID 15151435 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | 4-Methylenecyclohexylmethanol | HCID 13860 | — |
Reaction Steps
The reduction reaction of 4-methylene-cyclohexanecarboxylic acid ethyl ester with LAH is as described in the above reference. The product was purified by distillation to provide (4-methylene-cyclohexyl)-methanol as clear oil (3.67 g, 29.09 mmol, 50% over Step A and B).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07314872B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-67f1125e4fae4b4bb3bbea52a6e4ca48 |
| Source note | uspto-grants-2008_01 |