HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4,4a,9a-Tetrahydroanthracene-9,10-dione → HCID 18688925, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4,4a,9a-Tetrahydroanthracene-9,10-dione | HCID 92021 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 18688925 | HCID 18688925 | — |
| Product | 1,2,3,4,4a,9a-Hexahydroanthracene-9,10-dione | HCID 20509680 | — |
Reaction Steps
The operation is as in Example 1, except for using 63.6 g of 1,4,4a,9a-tetrahydro-anthraquinone, 150 cc of toluene and 0.4 g of palladium catalyst. After 3 hours at 80° C. under 100 bars pressure, 7 g of 1,2,3,4-tetrahydro-9,10-anthracene-diol and 57 g of 1,2,3,4,4a,9a-hexahydro-9,10-anthracene-dione are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04235666 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-1aefffd5a52a49589097a4e638caaf66 |
| Source note | uspto-grants-1980_11 |