HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-tert-Butylbenzaldehyde → 4-tert-Butyltoluene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-tert-Butylbenzaldehyde | HCID 70324 | — |
| Reactant | Benzenemethanol, 4-(1,1-dimethylethyl)-, 1-acetate | HCID 105421 | — |
| Product | 4-tert-Butyltoluene | HCID 7390 | 83.3% |
Reaction Steps
If the material discharged from the electrolysis is worked up similarly to Example 1, 284.8 g of p-tert.-butylbenzaldehyde and 295.3 g of p-tert.-butylbenzyl acetate are obtained in addition to 25.2 g of unconverted p-tert.-butyltoluene. This corresponds to a yield of 83.3% and a current efficiency of 58.2%. The p-tert.-butylbenzaldehyde is separated from the p-tert.-butylbenzyl acetate by the method described in Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04235683 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-5cac8f11e5494aa1bdf787d75a261d71 |
| Source note | uspto-grants-1980_11 |