4,5-Dichloro-1,2-phenylenediamine → HCID 22139850, compound

HRID 2250483Notes

Reaction equation

HRID 2250483 reaction equation
[CH3:1][C:2]1[C:3]([N:7]=[C:8]=[S:9])=[CH:4][S:5][CH:6]=1.[Cl:10][C:11]1[C:16]([Cl:17])=[CH:15][C:14]([NH2:18])=[C:13]([NH2:19])[CH:12]=1>>[NH2:19][C:13]1[CH:12]=[C:11]([Cl:10])[C:16]([Cl:17])=[CH:15][C:14]=1[NH:18][C:8]([NH:7][C:3]1[C:2]([CH3:1])=[CH:6][S:5][CH:4]=1)=[S:9]

Participants

3

Reactant 2

HCID 792974,5-Dichloro-1,2-phenylenediamineHCID 221398273-Isothiocyanato-4-methylthiophene

Product 1

HCID 22139850HCID 22139850, compound

Procedure

is obtained analogously to the reaction described in example 1 b) from 4-methyl-3-thienyl isothiocyanate and 4,5-dichloro-1,2-diaminobenzene. Crystalline solid, m.p. 310-320° C.

Workup

  1. customis obtained analogously to the reaction

Sources & evidence

ORD record
ord-5f12c283a4ae429caa0923d30cb44178
Source dataset
uspto-grants-2008_01
Patent number
US07317033B2

Reaction notes

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