Methyl iodide → HCID 131725761, compound

HRID 2250484Notes

Reaction equation

HRID 2250484 reaction equation
[NH2:1][C:2]1[CH:7]=[C:6]([Cl:8])[C:5]([Cl:9])=[CH:4][C:3]=1[NH:10][C:11]([NH:13][C:14]1[C:18]([CH3:19])=[CH:17][S:16][CH:15]=1)=S.CI>>[ClH:8].[Cl:9][C:5]1[C:6]([Cl:8])=[CH:7][C:2]2[N:1]=[C:11]([NH:13][C:14]3[C:18]([CH3:19])=[CH:17][S:16][CH:15]=3)[NH:10][C:3]=2[CH:4]=1

Participants

3

Reactant 2

HCID 6328Methyl iodideHCID 22139850HCID 22139850, compound

Product 1

HCID 131725761HCID 131725761, compound

Procedure

is obtained analogously to the procedure described in example 1 c) from N-(2-amino-4,5-dichlorophenyl)-N′-(4-methyl-3-thienyl)thiourea and methyl iodide. Crystalline solid, m.p. 290-294° C.

Workup

  1. customis obtained analogously to the procedure

Sources & evidence

ORD record
ord-315e2abd1f25469d85fe8dcc36c6030c
Source dataset
uspto-grants-2008_01
Patent number
US07317033B2

Reaction notes

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