3-Fluorobenzene-1,2-diamine → HCID 22139836, compound

HRID 2250486Notes

Reaction equation

HRID 2250486 reaction equation
[CH3:1][C:2]1[C:3]([N:7]=[C:8]=[S:9])=[CH:4][S:5][CH:6]=1.[F:10][C:11]1[C:12]([NH2:18])=[C:13]([NH2:17])[CH:14]=[CH:15][CH:16]=1>>[NH2:18][C:12]1[C:11]([F:10])=[CH:16][CH:15]=[CH:14][C:13]=1[NH:17][C:8]([NH:7][C:3]1[C:2]([CH3:1])=[CH:6][S:5][CH:4]=1)=[S:9]

Participants

3

Reactant 2

HCID 27828353-Fluorobenzene-1,2-diamineHCID 221398273-Isothiocyanato-4-methylthiophene

Product 1

HCID 22139836HCID 22139836, compound

Procedure

is obtained analogously to the reaction described in example 1 b) from 4-methyl-3-thienyl isothiocyanate and 3-fluoro-1,2-diaminobenzene. Crystalline solid, point of decomposition >240° C.

Workup

  1. customis obtained analogously to the reaction
  2. customCrystalline solid, point of decomposition >240° C.

Sources & evidence

ORD record
ord-590a0b9bb90e4d8f9c9c66587c839bdc
Source dataset
uspto-grants-2008_01
Patent number
US07317033B2

Reaction notes

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