2,3-Diaminotoluene → HCID 22139806, compound

HRID 2250489Notes

Reaction equation

HRID 2250489 reaction equation
[CH3:1][C:2]1[C:3]([N:7]=[C:8]=[S:9])=[CH:4][S:5][CH:6]=1.[CH3:10][C:11]1[C:12]([NH2:18])=[C:13]([NH2:17])[CH:14]=[CH:15][CH:16]=1>>[NH2:18][C:12]1[C:11]([CH3:10])=[CH:16][CH:15]=[CH:14][C:13]=1[NH:17][C:8]([NH:7][C:3]1[C:2]([CH3:1])=[CH:6][S:5][CH:4]=1)=[S:9]

Participants

3

Reactant 2

HCID 175932,3-DiaminotolueneHCID 221398273-Isothiocyanato-4-methylthiophene

Product 1

HCID 22139806HCID 22139806, compound

Procedure

is obtained analogously to the reaction described in example 1 b) from 4-methyl-3-thienyl isothiocyanate and 3-methyl-1,2-diaminobenzene. Crystalline solid, m.p. 184-186° C.,

Workup

  1. customis obtained analogously to the reaction

Sources & evidence

ORD record
ord-b223eeafd63744bd93e69869af1c32aa
Source dataset
uspto-grants-2008_01
Patent number
US07317033B2

Reaction notes

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