1,2-Diaminocyclohexane, trans- → HCID 87458895, compound

HRID 2250490Notes

Reaction equation

HRID 2250490 reaction equation
[CH3:1][C:2]1[C:3]([N:7]=[C:8]=[S:9])=[CH:4][S:5][CH:6]=1.[NH2:10][C@@H:11]1[CH2:16][CH2:15][CH2:14][CH2:13][C@H:12]1[NH2:17]>>[NH2:10][C@@H:11]1[CH2:16][CH2:15][CH2:14][CH2:13][C@H:12]1[NH:17][C:8]([NH:7][C:3]1[C:2]([CH3:1])=[CH:6][S:5][CH:4]=1)=[S:9]

Participants

3

Reactant 2

HCID 438061,2-Diaminocyclohexane, trans-HCID 221398273-Isothiocyanato-4-methylthiophene

Product 1

HCID 87458895HCID 87458895, compound

Procedure

is obtained analogously to the reaction described in example 1 b) from 4-methyl-3-thienyl isothiocyanate and racemic trans-1,2-diaminocyclohexane. Crystalline solid, m.p. 205-210° C.,

Workup

  1. customis obtained analogously to the reaction

Sources & evidence

ORD record
ord-2fcaee80358b43d58c9506c96730c10f
Source dataset
uspto-grants-2008_01
Patent number
US07317033B2

Reaction notes

Loading…