Benzo(d)thiazol-2-amine → HCID 8379104, compound

HRID 2250670Notes

Reaction equation

HRID 2250670 reaction equation
[NH2:1][C:2]1[S:3][C:4]2[CH:10]=[CH:9][CH:8]=[CH:7][C:5]=2[N:6]=1.[S:11]1[C:15]([C:16](Cl)=[O:17])=[CH:14][C:13]2[CH:19]=[CH:20][CH:21]=[CH:22][C:12]1=2>N1C=CC=CC=1>[S:3]1[C:4]2[CH:10]=[CH:9][CH:8]=[CH:7][C:5]=2[N:6]=[C:2]1[NH:1][C:16]([C:15]1[S:11][C:12]2[CH:22]=[CH:21][CH:20]=[CH:19][C:13]=2[CH:14]=1)=[O:17]

Participants

4

Reactant 2

HCID 8706Benzo(d)thiazol-2-amineHCID 142384Benzo[b]thiophene-2-carbonyl Chloride

Product 1

HCID 8379104HCID 8379104, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

Using 2-amino-benzothiazole and benzo[b]thiophene-2-carboxylic acid chloride in pyridine the title compound was obtained as a light yellow solid (86% yield), MS: m/e=311.1 (M+H+).

Sources & evidence

ORD record
ord-e88a1f0c43484854a3343449ac3bf052
Source dataset
uspto-grants-2008_01
Patent number
US07317007B2

Reaction notes

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