Benzo(d)thiazol-2-amine → HCID 1245575, compound

HRID 2250672Notes

Reaction equation

HRID 2250672 reaction equation
[NH2:1][C:2]1[S:3][C:4]2[CH:10]=[CH:9][CH:8]=[CH:7][C:5]=2[N:6]=1.[CH3:11][C:12]1[S:16][C:15]([C:17](Cl)=[O:18])=[CH:14][CH:13]=1>N1C=CC=CC=1>[S:3]1[C:4]2[CH:10]=[CH:9][CH:8]=[CH:7][C:5]=2[N:6]=[C:2]1[NH:1][C:17]([C:15]1[S:16][C:12]([CH3:11])=[CH:13][CH:14]=1)=[O:18]

Participants

4

Reactant 2

HCID 8706Benzo(d)thiazol-2-amineHCID 27600835-Methylthiophene-2-carbonyl chloride

Product 1

HCID 1245575HCID 1245575, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

Using 2-amino-benzothiazole and 5-methyl-thiophene-2-carboxylic acid chloride in pyridine the title compound was obtained as a yellow solid (87% yield), MS: m/e=275.1 (M+H+).

Sources & evidence

ORD record
ord-331bf8b07b374a43b42f47eada6be9c4
Source dataset
uspto-grants-2008_01
Patent number
US07317007B2

Reaction notes

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