HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → 3-Nitro-5-pentafluorosulfanylbenzoic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 3-(Pentafluorosulfanyl)benzoic acid | HCID 2779209 | — |
| Product | 3-Nitro-5-pentafluorosulfanylbenzoic Acid | HCID 59642152 | — |
Reaction Steps
4.0 g of 3-pentafluorosulfanylbenzoic acid were dissolved at RT in 50 ml of 100% HNO3 and 10 ml of H2SO4 were added with ice cooling. The mixture was stirred at RT for 6 days, then poured onto 200 g of ice and stirred for a further hour, and finally the product was filtered off with suction. 4.4 g of bright yellow crystals were obtained, m.p. 140° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07317124B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-cea335b4ab0d43f2aabf8a2465d5f6f4 |
| Source note | uspto-grants-2008_01 |