Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diethanolamine | HCID 8113 | — |
| Reactant | Diglycidyl ether | HCID 16704 | — |
| Reactant | 2-Ethylhexyl glycidyl ether | HCID 17162 | — |
| Product | HCID 59000137 | HCID 59000137 | — |
Reaction Steps
A three-necked, septum capped, 250 mL, round-bottom flask equipped with an addition funnel and containing a magnetic stirring bar is flushed with argon and charged with 2-ethylhexylglycidyl ether (66.53 g, 0.35 mol). Diethanolamine (40.89 g, 0.38 mol) is added during 10 min to the glycidyl ether, with stirring. The flask is placed in an oil bath and heated at a bath temperature of 75-80° C. overnight. The reaction is cooled and checked by 1H NMR to ensure the complete consumption of the glycidyl ether. A colorless viscous liquid is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07318843B2 |
|---|
| Source dataset | uspto-grants-2008_01 |
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| ORD ID | ord-a00a63a051a2468798f0be96db48ff92 |
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| Source note | uspto-grants-2008_01 |
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