Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2250980Generated: October 31, 2026

Picolyl chloride → HCID 69200917, compound

https://huagongshe.com/reaction/2250980

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPicolyl chlorideHCID 23393—
ReactantHCID 14631438HCID 14631438—
ProductHCID 69200917HCID 6920091721%

Reaction Steps

Methyl-2-tert-butoxycarbonylamino-3-(3,5-dibromo-4-hydroxyphenyl)propionate (0.035 mmol) was coupled with 2-chloromethylpyridine and hydrolyzed using the method described in “General procedure for the preparation of Examples 8-22”. This gave 21% yield of 2-amino-3-[3,5-dibromo-4-(pyridin-2-ylmethoxy)phenyl]propionate triethylammonium. LC/MS (electrospray): m/z 429 (M−1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07319096B2
Source datasetuspto-grants-2008_01
ORD IDord-bded5680f5ca4cb0b5da3d599fad6792
Source noteuspto-grants-2008_01