HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Chloromethyl)pyridine → HCID 69199813, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Chloromethyl)pyridine | HCID 74571 | — |
| Reactant | HCID 14631438 | HCID 14631438 | — |
| Product | HCID 69199813 | HCID 69199813 | 13% |
Reaction Steps
Methyl-2-tert-butoxycarbonylamino-3-(3,5-dibromo-4-hydroxyphenyl)propionate (0.035 mmol) was coupled with 4-chloromethylpyridine and hydrolyzed using the method described in “General procedure for the preparation of Examples 8-22”. This gave 13% yield of 2-amino-3-[3,5-dibromo-4-(pyridin-4-ylmethoxy)phenyl]propionate triethylammonium. LC/MS (electrospray): m/z 429 (M−1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07319096B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-7f160f9840444882a70e486d53af9dc4 |
| Source note | uspto-grants-2008_01 |