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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2250984Generated: November 1, 2026

3-Iodobenzyl bromide → HCID 10231138, compound

https://huagongshe.com/reaction/2250984

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-Iodobenzyl bromideHCID 2759361—
ReactantHCID 14631438HCID 14631438—
ProductHCID 10231138HCID 1023113838%

Reaction Steps

Methyl-2-tert-butoxycarbonylamino-3-(3,5-dibromo-4-hydroxyphenyl)propionate (0.035 mmol) was coupled with 1-bromomethyl-3-iodobenzene and hydrolyzed using the method described in “General procedure for the preparation of Examples 8-22”. This gave 38% yield of 2-amino-3-[3,5-dibromo-4-(3-iodobenzyloxy)phenyl]propionic acid. LC/MS (electrospray): m/z 554 (M−1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07319096B2
Source datasetuspto-grants-2008_01
ORD IDord-0a83b65f3fc6476881f1cdf43115e57a
Source noteuspto-grants-2008_01