Pyrazol-3-ylamine → HCID 178515162, compound

HRID 2251108Notes

Reaction equation

HRID 2251108 reaction equation
[N:1]1[N:9]2[C:4]([N:5]=[C:6]3[CH2:15][CH2:14][CH2:13][CH2:12]C[C:7]3=[C:8]2[OH:10])=[CH:3][CH:2]=1.COC(C1CCCCC1=O)=O.N1NC(N)=CC=1>C(O)(=O)C>[N:1]1[N:9]2[C:4]([N:5]=[C:6]3[C:7](=[C:8]2[OH:10])[CH2:12][CH2:13][CH2:14][CH2:15]3)=[CH:3][CH:2]=1

Participants

5

Reactant 3

HCID 74561Pyrazol-3-ylamineHCID 170489Cyclohexanecarboxylic acid, 2-oxo-, methyl esterHCID 178515163HCID 178515163, compound

Product 1

HCID 178515162HCID 178515162, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

Using the method described for the preparation of 6,7,8,9-tetrahydro-5H-1,4,10a-triaza-cyclohepta[f]inden-10-ol, the reaction of 2-oxo-cyclohexanecarboxylic acid methyl ester and 2H-pyrazol-3-ylamine in acetic acid provided the title compound.

Sources & evidence

ORD record
ord-e1d382202aa34705a1733bde84fa0b11
Source dataset
uspto-grants-2008_01
Patent number
US07319103B2

Reaction notes

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